High-temperature supersonic molecular-beam source
- 1 August 1992
- journal article
- Published by AIP Publishing in Review of Scientific Instruments
- Vol. 63 (8) , 3939-3943
- https://doi.org/10.1063/1.1143242
Abstract
We describe a supersonic molecular-beam source that can be heated to over 2300 K. Our design employs a commercially available tungsten tube which is resistively heated by passage of current along its length between two water-cooled copper clamps. The clamps are supported so as to minimize bending stresses on the tube while allowing for thermal expansion. Gas is supplied to the tube at one end using an o-ring connection and emerges from an orifice drilled about halfway along the length. The other end of the tube is welded closed. Temperature is measured by a thermocouple spot-welded adjacent to the orifice. The entire tube is surrounded by two tantalum heat shields which are split lengthwise for convenient assembly. These have large holes aligned with the beam axis. We present details of the design, assembly, and characterization of this source.Keywords
This publication has 13 references indexed in Scilit:
- Formation of silver clusters in nozzle expansionsThe European Physical Journal D, 1991
- A search for vibrational contributions to the activated adsorption of H2 on copperChemical Physics Letters, 1990
- Coupled translational-vibrational activation in dissociative hydrogen adsorption on Cu(110)Physical Review Letters, 1989
- Promotion of dissociative chemisorption with vibrational and translational energyJournal of Vacuum Science & Technology A, 1988
- Laser induced excitation spectroscopy of copper trimer in various stages of supersonic expansion: Observation of fluorescence from dissociative levelsThe Journal of Chemical Physics, 1986
- Laser Spectroscopy of Cold Gas-Phase MoleculesAnnual Review of Physical Chemistry, 1980
- The supersonic expansion of pure copper vaporThe Journal of Chemical Physics, 1979
- Molecular optical spectroscopy with supersonic beams and jetsAccounts of Chemical Research, 1977
- The Hyperfine Structure of theState of. The Nuclear Electric Quadrupole MomentPhysical Review B, 1949
- A Tungsten Furnace for Experiments on Dissociation and IonizationJournal of the Optical Society of America, 1922