IMMUNOCHEMISTRY OF I/I-ACTIVE OLIGOSYLCERAMIDES AND POLYGLYCOSYLCERAMIDES FROM RABBIT ERYTHROCYTE-MEMBRANES - CHARACTERIZATION OF LINEAR, DIANTENNARY, AND TRIANTENNARY NEOLACTOGLYCOSPHINGOLIPIDS
- 1 January 1985
- journal article
- research article
- Vol. 260 (8) , 4927-4935
Abstract
A triantennary ceramide pentadecasaccharide (BIrab-2) with blood group I and B-like activity and an unbranched ceramide heptasaccharide (Birab) with i- and B-like activity were isolated in high yield from rabbit erythrocyte membranes. The structures of the native substances and the products obtained after treatment with .alpha.-galactosidase (BIrab-2.alpha., Birab.alpha.) and subsequent Smith degradation (BIrab-2.alpha.SD) were determined by sugar analysis, methylation analysis, and fast atom bombardment-mass spectrometry of the permethylated derivatives. Together with the results of 1H NMR analysis structures were established for the native substances.This publication has 2 references indexed in Scilit:
- Characterization of GM1 ganglioside by direct inlet chemical ionization mass spectrometry.Journal of Lipid Research, 1982
- The application of mass spectrometry in the structural elucidation of glycosphingolipidsChemistry and Physics of Lipids, 1978