Abstract
The hybrid phases Nb59O147F and Nb65O161F3 were prepared at high temperature and investi­gated by high resolution transmission electron microscopy. Both phases have block structures. The sample of the phase Nb59O147F is very well ordered, whereas the phase Nb65O161F3 shows some defects. In a sample of Nb65O161F3 microdomains of a new 2:1 hybrid phase Nb96O238F4 were found. Structural differences of the systems Nb2O5/NbO2F and Nb2O5/WO3 are discussed.

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