The crystal structure of tert- butyl ethyldiazoacetate mercury(II)
- 15 July 1977
- journal article
- Published by Canadian Science Publishing in Canadian Journal of Chemistry
- Vol. 55 (14) , 2752-2754
- https://doi.org/10.1139/v77-383
Abstract
Tert-Butyl ethyldiazoacetate mercury(II) is monoclinic with the following unit cell data at 20 °C: P21/n, a = 8.089(3), b = 18.720(10), c = 7.893(3) Å, β = 93.20(3)°, V = 1193.3 Å3, ρo = 2.09(1), ρc = 2.06, Z = 4. The structure was solved by heavy atom methods and refined to R = 6.6% for 1003 reflections. The diazoacetate portion is planar; the CN2 portion is linear.Keywords
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