[HRu6(CO)18]: a ruthenium anion having an interstitial H-ligand. X-Ray crystal structures of two modifications

Abstract
Reaction of [Ru3(CO)12] with [Mn(CO)5] gives [Ru6(CO)18]2– which on acidification is converted into [HRu6(CO)18]; this monoanion has spectroscopic properties and an X-ray structure consistent with the H ligand lying at the centre of an octahedron (approximating to Oh symmetry) of ruthenium atoms.

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