Crystal structure of 1-hydroxymethyl-4-methyl-7-oxabicyclo[4,3,0]non-4-en-8-one
- 1 January 1973
- journal article
- research article
- Published by Royal Society of Chemistry (RSC) in Journal of the Chemical Society, Perkin Transactions 2
- No. 3,p. 240-243
- https://doi.org/10.1039/p29730000240
Abstract
Crystals of the title compound are monoclinic, a= 7·973, b= 6·249, c= 9·444 Å, β= 95·8°, Z= 2, with space group P21. The structure was determined from diffractometer data by direct methods, and refined by full-matrix least-squares to R 0·068 for 681 data. The two rings are cis-fused and the molecules are hydrogen-bonded in chains parallel to the a axis. Bond lengths and angles are generally normal.Keywords
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