Electron Excitation and Chemical Steps during Anodic Decomposition of n‐GaAs Electrodes: A Hole Injection Study

Abstract
The contribution of electron excitation to the anodic dissolution of the n‐GaAs electrode was studied quantitatively by measuring the increase in the anodic blocking current when hole‐injecting agents such as Ce4+ or Fe(CN)3−6 were added to the electrolyte solution. The experimental relationship between the anodic current and the cathodic hole injection current was interpreted on the basis of the anodic decomposition mechanism, including a chemical step, proposed previously to explain stabilization results. This mechanism is complemented by an electrochemical step involving electron excitation from a decomposition intermediate occurring in parallel to the chemical step.

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