New Sulfur‐ and Selenium‐Bridged Copper Clusters; Ab Initio Calculations on [Cu2nSen(PH3)m] Clusters

Abstract
The synthesis of new, medium‐sized copper clusters with unusual structures and a successful combination of experiment and theoretical calculation—this is offered by the present communication. The reaction of CuAc with PR2R′ (R, R′  Et, Ph) and E(SiMe3)2 (E  S, Se) leads to the clusters 1–4. Several of these might be intermediates in the synthesis of larger cluster complexes. The structure of [Cu12Se6(PH3)8] calculated by ab initio methods agrees with the structure of 1 within the limits of the methods. equation image
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