Abstract
A hitherto undescribed mold metabolic product, dihydrogladiolic acid, was isolated from culture filtrates of P. gladioli grown on a modified Raulin-Thom solution. It is believed to be 5-formyl-6-hydroxymethyl-2-methoxy-3-methylbenzoic acid. Physical and chemical properties were detd. Dihydrogladiolic acid is readily oxidized in vitro to gladiolic acid by heating with KIO4 in dilute sulfuric acid soln. Gladiolic acid is believed to be 5,6-diformyl-2-methoxy-3-methylbenzoic acid, or its tautomer. Cyclopolic and cyclopaldic acids from P. cyclopium are thus 4-hydroxydihydrogladiolic acid and 4-hydroxygladiolic acid, respectively.
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