Burgers vector determination of decorated dislocations in γ-TiAl by diffraction contrast and large-angle convergent-beam electron diffraction

Abstract
Decorated and undecorated dislocations in γ-TiAl have been studied by conventional transmission electron microscopy using diffraction contrast and by large-angle convergent-beam electron diffraction (LACBED). The results of the Burgers vector determination for undecorated and decorated dislocations using the different techniques have been compared. For the decorated dislocations the contrast from the decorating particles and the underlying dislocation have been separated and the misfit introduced by the precipitates has been determined. Computer simulations of the contrast from decorated dislocations in LACBED patterns have been performed. The rules governing the dislocation contrast in LACBED patterns have been discussed and extended to the case of decorated dislocations. A new fringe-counting rule to determine the Burgers vectors of dislocations decorated by misfitting precipitates has been proposed. Remarkably good agreement of the computer-simulated LACBED contrast with experimental observations has been achieved.