Synthesis of TiNF and Structure Determination by Powder Diffraction using Synchrotron Radiation
- 1 July 1988
- journal article
- research article
- Published by Wiley in Angewandte Chemie International Edition in English
- Vol. 27 (7) , 929-930
- https://doi.org/10.1002/anie.198809291
Abstract
An unproblematic determination of the structure of the pseudooxide TiNF, a light green to olive green, air stable and chemically substantially inert powder, has been achieved by synchroton‐powder diffraction. TiNF has an anatase structure and does not exhibit any superstructure, even according to electron‐microscopic findings. TiNF was synthesized by ammonolysis of activated (NH4)2TiF6 with a stream of dry, O2‐free NH3.Keywords
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