Abstract
Essential oils from citrus peels were extracted and separated with CO2 under supercritical conditions in a single process. The peels were placed together with ethanol, as an entraining solvent, inside a high pressure cell filled with carbon dioxide at a pressure < 130 bar and a temperature of 35°C. The extract was fractionated in various pressure ranges after achieving equilibrium, and it was analyzed with a gas chromatograph. The initial fraction contained most of the water content of the peels while the following fractions were rich in essential oils. A mechanism for the extraction and separation is also given.

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