Micro-scale Synthesis andIn-SituSpectroscopic Characterization of Some Chemical Weapons Related Organophosphonate Compounds
- 1 June 1998
- journal article
- research article
- Published by Taylor & Francis in Analytical Letters
- Vol. 31 (8) , 1429-1444
- https://doi.org/10.1080/00032719808002877
Abstract
Inspection protocols for the Chemical Weapons Treaty, which went into effect on April 29, 1997 require on-site analytical procedures which include a comprehensive mass spectral database of hundreds of scheduled compounds. A number of these compounds were prepared on a nanogram scale via a micro-scale synthetic approach using GC-IRD/MSD analytical instrumentation to purify and identify the resulting products. The collected electron impact mass spectra will be made available for use in relevant databases.Keywords
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