Gas-Liquid Chromatographic Analysis of Long-Chain Fatty Alcohols
Open Access
- 31 January 1968
- journal article
- research article
- Published by Oxford University Press (OUP) in Journal of Chromatographic Science
- Vol. 6 (2) , 94-96
- https://doi.org/10.1093/chromsci/6.2.94
Abstract
Trifluoroacetate (TFA) and trimethylsilyl ether (TMS) derivatives of fatty alcohols ranging in chain length from C14 to C20 were analyzed by gas-liquid chromatography. The TFA and TMS derivatives gave quantitative results for both saturated and unsaturated standard mixtures. Excellent resolution of the TFA derivatives on the polar liquid phase allows quantitation of mixtures containing both saturated and unsaturated alcohols. Analyses were carried out on columns (5-ft × 1/8-in) containing 15% ethylene glycol succinate methyl silicone polymer (EGSS-X) and 5% methyl silicone polymer (SE-30) liquid phases operated at 130° and 190°C, respectively, for both derivatives.This publication has 6 references indexed in Scilit:
- Characterization and identification of glyceryl ether diesters present in tumor cellsJournal of Lipid Research, 1967
- Chemical and physical properties of isomeric glyceryl monoethersLipids, 1967
- Metabolism of alpha‐alkoxy glyceryl monoethers in rat liver, in vivo and in vitroLipids, 1966
- Chemical composition of the wax secreted by a scale insect (Ceroplastes pseudoceriferus Green)Lipids, 1966
- Reactions of dimethyl sulfoxide with sulfonate esters of fatty alcohols. I. Synthesis of higher saturated and unsaturated fatty aldehydesLipids, 1966
- Gas‐liquid chromatographic analysis of long chain isomeric glyceryl monoethersLipids, 1966