A Fast X-Ray Absorption Spectrometer for Use with Synchrotron Radiation

Publisher Website
Google Scholar
Abstract
A quasi-parallel and polychromatic beam of synchrotron radiation is focused and dispersed by a curved crystal, so that the energy of each ray of the focused beam varies as a function of convergence angle through the focus. The specimen is placed at the focus. By measuring the X-ray intensity distribution across the beam behind the focus, in the presence and absence of the specimen, the absorption spectra of Cu and Ni metal foils were obtained. Using an X-ray film as the detector, a spectrum from a Cu foil was obtained in 0.1 seconds when the SPEAR storage ring at Stanford was operated at 3.1 GeV and 80 mA. The energy resolution is approximately 2.0 eV and the energy range of the spectrum is approximately 1 keV.